首页 > 过刊浏览>2021年第29卷第1期 >96-104. DOI:10.11926/jtsb.4256
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杭白菊花水提物的UHPLC-ESI-Orbitrap质谱联用分析
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福建省重大专项专题项目（2018NZ0003-2）；福建省农业科学院科技创新团队建设项目（STIT2017-2-11）资助


Chemical Constituents of Water Extract from Chrysanthemum morifolium Flowers by UHPLC-ESI-Orbitrap MS
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    摘要:

    为阐明杭白菊花水提物的药效物质基础，采用超高压液相-高分辨质谱联用技术对杭白菊（Chrysanthemum morifolium）花水提物的化学成分进行分析和鉴定。结果表明，从杭白菊花水提物中鉴定出376种化学成分，其中相对含量大于0.1%的成分有152种，相对含量较高的有绞股蓝皂苷XXVII、含羞草碱-O-β-葡萄糖苷、甲基-β-葡萄糖苷、d-1-O-甲基粘质肌醇、l（+）-甲基肌醇、过氧化苯甲酰、甲基-β-半乳糖苷、甲基-α-果糖苷、芒柄醇、松醇、（E）-2-己烯-α-阿拉伯糖-（1→2）-β-葡萄糖苷、米瑟毒苷等。杭白菊花水提物主要以黄酮类和生物碱类成分为主，分别有40和53种，相对含量分别为22.68%和26.57%，是杭白菊花发挥功效的主要物质基础。

    Abstract:

    In oreder to understand the effective substances of water extract from Chrysanthemum morifolium flowers, its chemical constituents were identified by high-pressure liquid chromatography-high resolution mass spectrometry. The results showed that 376 chemical components were identified from flower water extract, and the relative content of 152 components were more than 0.1%. The components with high relative content included gypenoside XXVII, mimosine-O-β-glucoside, methyl-β-glucoside, d-1-O-methyl mucoinositol, l(+)-bornesitol, lucidol, methyl-β-galactoside, methyl-α-fructoside, ononitol, pinitol, (E)-2-hexenyl-α-arabinosyl-(1→2)-β-glucoside, miserotoxin, and so on. Therefore, the maim constituents in flower water extract of C. morifolium were flavonoids and alkaloids, which had 40 and 53 kinds with relative content of 22.68% and 26.57%, respectively, indicating that the main material basis for the performance of C. morifolium flowers.

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徐晓俞,李程勋,郑开斌,李爱萍.杭白菊花水提物的UHPLC-ESI-Orbitrap质谱联用分析[J].热带亚热带植物学报,2021,29(1):96~104

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  • 收稿日期:2020-05-26
  • 最后修改日期:2020-07-10
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