卢旺达产迷迭香化学成分研究I
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天津中医药大学 天津市中药化学与分析重点实验室,天津中医药大学 天津市中药化学与分析重点实验室,天津中医药大学 天津市中药化学与分析重点实验室,天津中医药大学 天津市中药化学与分析重点实验室,天津中医药大学 天津市中药化学与分析重点实验室,天津中医药大学 天津市中药化学与分析重点实验室

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New Century Excellent Talents in University (NCET-12-1069), Program for Tianjin Innovative Research Team in University (TD12-5033)


Chemical Constituents from Rwandan Plant Rosmarinus officinalis L. (I)
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Key Laboratory of Traditional Chinese Medicinal Chemistry and Analytical Chemistry of Tianjin,Key Laboratory of Traditional Chinese Medicinal Chemistry and Analytical Chemistry of Tianjin,Key Laboratory of Traditional Chinese Medicinal Chemistry and Analytical Chemistry of Tianjin,Key Laboratory of Traditional Chinese Medicinal Chemistry and Analytical Chemistry of Tianjin,Key Laboratory of Traditional Chinese Medicinal Chemistry and Analytical Chemistry of Tianjin,Key Laboratory of Traditional Chinese Medicinal Chemistry and Analytical Chemistry of Tianjin

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    摘要:

    为了解迷迭香(Rosmarinus officinais L.)中的化学成分,从其95% 乙醇提取物中分离得到了13 种化合物,经波谱分析,分别鉴定为(Z)-3-hexenyl glucoside (1),(Z)-3-hexenyl O-β-D-glucopyranosyl-(1''→6')-β-D-glucopyranoside (2),erythritol-1-O-(6-Otrans-caffeoyl)-β-D-glucopyranoside (3),2,3,4,5-tetrahydroxyhexyl-6-O-trans-caffeoyl-β-glucopyranoside (4), 1,2,3,4-tetrahydroxy-2-methylbutane-4-O-(6-O-trans-caffeoyl)-β-D-glucopyranoside (5),咖啡酸 (6),迷迭香酸 (7),methyl rosmarinate (8),methylbenzoate-4-β-glucoside (9),benzyl-β-D-glucopyranoside (10),benzyl-O-β-D-apiofuranosyl-(1→2)-β-D-glucopyranoside (11),1,2-di-O-β-D-glucopranosyl-4-allylbenzene (12)及(+)-syringaresinol-4'-O-β-D-glucopyranoside (13).其中,化合物1~58~13 为首次从迷迭香属分离得到,并修正了化合物13 的波谱数据.

    Abstract:

    In order to understand the chemical constituents of Rosmarinus officinalis, 13 compounds were isolated from its 95% EtOH extract. On the basis of spectral data, their structures were identified as (Z)-3- hexenyl glucoside (1), (Z)-3-hexenyl O-β-D-glucopyranosyl-(1''→6')-β-D-glucopyranoside (2), erythritol-1-O- (6-O-trans-caffeoyl)-β-D-glucopyranoside (3), 2,3,4,5-tetrahydroxyhexyl-6-O-trans-caffeoyl-β-glucopyranoside (4), 1,2,3,4-tetrahydroxy-2-methylbutane-4-O-(6-O-trans-caffeoyl)-β-D-glucopyranoside (5), caffeic acid (6), rosmarinic acid (7), methyl rosmarinate (8), methyl benzoate-4-β-glucoside (9), benzyl-β-D-glucopyranoside (10), benzyl-O-β-D-apiofuranosyl-(1→2)-β-D-glucopyranoside (11), 1,2-di-O-β-D-glucopranosyl-4-allylbenzene (12) and (+)-syringaresinol-4'-O-β-D-glucopyranoside (13). Among them, compounds 1-5 and 8-13 were isolated from the Rosmarinus genus for the first time. For the known ones, the NMR data of compound 13 was corrected.

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TIWALADE Adegoke Adelakun,李晓霞,瞿璐,陈玥,王涛,张祎.卢旺达产迷迭香化学成分研究I[J].热带亚热带植物学报,2015,23(3):310~316

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  • 收稿日期:2014-07-28
  • 最后修改日期:2014-09-16
  • 录用日期:2014-11-14
  • 在线发布日期: 2015-05-21
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